3,4-Diphenyl-2,5-bis(trimethylsilyl)cyclopentadienone
نویسندگان
چکیده
منابع مشابه
25-34 Aldridge
We reviewed the historic and present distribution of Greater Sage-Grouse (Centrocercus urophasianus) in Canada and found that the species has been eliminated from approximately 90% of its estimated historic distribution. Sage-grouse have been extirpated from British Columbia and reduced to remnant populations in Alberta and Saskatchewan. Estimates of the size of the population decline in Canada...
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The complete mol-ecule of the title compound, C(12)H(10)ClO(2)PS, is generated by crystallographic mirror symmetry, with the P, S and Cl atoms lying on the mirror plane. The resulting PO(2)SCl tetra-hedron is significantly distorted [O-P-O = 96.79 (9)°]. The crystal packing exhibits no directional inter-actions.
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The title compound, C40H41NO8, is a product of the reduction of the cyclic carbonyl group of the γ-piperidone subunit of the aza-14-crown-4 ether with subsequent re-esterification of its dimethyl butenoate substituent into a monoethyl monomethyl group. The aza-crown macrocycle exhibits a bowl conformation with a dihedral angle of 70.82 (5)° between the benzene rings fused to it. The piperidine ...
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The title compound, C(39)H(37)NO(8), is a product of the Michael addition of the cyclic secondary amine subunit of aza-14-crown-4 ether to dimethyl acetyl-enedicarboxyl-ate. The piperidinone ring exhibits a distorted chair conformation and the dimethyl acetyl-enedicarboxyl-ate fragment has a cis configuration with a dihedral angle of 56.61 (5)° between the two carboxyl-ate groups. The crystal p...
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The P atom in the title compound, C(19)H(18)NO(3)P, exhibits a distorted tetra-hedral configuration while the N atom shows a planar coordination. In the crystal, inter-molecular N-H⋯O hydrogen bonds form centrosymmetric dimers.
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ژورنال
عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online
سال: 2008
ISSN: 1600-5368
DOI: 10.1107/s1600536808032923